Simultaneous Spectrophotometric Determination of Amlodipine and Metoprolol by Principal Component Regression Multivariate Calibration and Comparison with HPLC

Authors

Mohsen Shahlaei1, Farshid Hassanzadeh2, Jaber Emami3, Ehsan Sohrabi2, Lotfollah Saghaie2,*
1Medical Biology Research Center, Kermanshah University of Medical Sciences, Kermanshah, Iran
2Department of Medicinal Chemistry, Faculty of Pharmacy and Pharmaceutical sciences, Isfahan University of Medical Sciences, 81746-73461 Isfahan, Iran
3Department of Pharmaceutics, Faculty of Pharmacy and Pharmaceutical sciences, Isfahan University of Medical Sciences, 81746-73461 Isfahan, Iran
*Corresponding Author: Corresponding author: Department of Medicinal Chemistry, Faculty of Pharmacy and Pharmaceutical sciences, Isfahan University of Medical Sciences, 81746-73461 Isfahan, Iran. Email:[email protected]

Journal of Reports in Pharmaceutical Sciences:Vol. 2, issue 2; 179-189
Published online:Dec 20, 2013
Article type:Research Article
Received:Oct 19, 2013
Accepted:Nov 09, 2013
How to Cite:Shahlaei M, Hassanzadeh F, Emami J, Sohrabi E, Saghaie L. Simultaneous Spectrophotometric Determination of Amlodipine and Metoprolol by Principal Component Regression Multivariate Calibration and Comparison with HPLC. J Rep Pharm Sci. 2013;2(2):e147753. doi:

Abstract

Multi-drug therapy in high blood pressure is appreciated to achieve a normal blood pressure. A simple spectrophotometric method based on principal component analysis has been proposed for simultaneous determination of amlodipine (Amd) and metoprolol (Met) in pharmaceutical preparations. Calibration matrix contains 3.402 μgml-1 to 170.130 μg ml-1 amlodipine and 13.7 μg ml-1 to 68.5 μgml-1 metoprolol. The proposed method was validated by using a set of synthetic sample mixtures and subsequently applied to simultaneous determination of amlodipine and metoprolol in different pharmaceutical preparations. 

Highlights

Copyright

© 2013, Author(s). This open-access article is available under the Creative Commons Attribution 4.0 (CC BY 4.0) International License (https://creativecommons.org/licenses/by/4.0/), which allows for unrestricted use, distribution, and reproduction in any medium, provided that the original work is properly cited.

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